Critical Analysis and Development.

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GuingesRock
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Re: Critical Analysis and Development.

Post by GuingesRock » Mon Aug 26, 2013 8:20 am

I don't know. It was really nice 4 weeks ago, but over the past two weeks, more and more, I have been liking it less.

Sorry to hear about your beer. If you can't sort it out you could call the Brewnosers Swat team... I did, and they came screeching to the door, sirens, flashing lights and all, and sorted out my beer. I still can't believe that happened. I can now feel relaxed in my own home.

"Experience is cheap at any price" as my father used to say. I now have a lot of experience with high fermentation temperatures.

Good luck.

:)
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Re: Critical Analysis and Development.

Post by CartoonCod » Mon Aug 26, 2013 10:56 am

No worries Mark, thank you for having us over, that blast of fresh hops from your real ale was just what I needed on a warm Sunday afternoon.

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Re: Critical Analysis and Development.

Post by Jayme » Tue Aug 27, 2013 3:14 pm

Just reading this thread and have a few comments on things mentioned a while back.

When it comes to diacetyl, I personally find it reminds me more of butterscotch than popcorn - I think everyone perceives it somewhat differently though. The other thing that I find with diacetyl is sometimes I can only detect it on the nose, sometimes only through taste (sometimes both), but the one indicator that never seems to let me down is mouth feel. There is a slippery/slick feeling that comes with diacetyl.

Also, there was talk about solid state cooling. I have a fridge that is pretty much the EXACT right size for a carboy and works great (runs of 110V, though there's definitely a regulator converting to DC). I have been searching high and low for one since - I've found a smaller version, but it would seem I've got the only one ever built of this size! I'm sure that's not the case, but it sure seems like it haha. Since then, I've bought a couple of the round gatorade coolers. They use a traditional compressor, but carboys fit well and they don't take up too much space.

Lastly, I've been meaning to start organizing beer feedback for those who are seeking it. Essentially the idea is to gather beer and on a semi-regular basis, get all my fellow BJCP folks together to judge them. We only wrote the exam in May and the summer has been nuts, but I'm hoping once things calm down in the fall, I can get something started.
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Re: Critical Analysis and Development.

Post by GuingesRock » Tue Aug 27, 2013 7:45 pm

Jayme wrote: Lastly, I've been meaning to start organizing beer feedback for those who are seeking it. Essentially the idea is to gather beer and on a semi-regular basis, get all my fellow BJCP folks together to judge them. We only wrote the exam in May and the summer has been nuts, but I'm hoping once things calm down in the fall, I can get something started.
I would really appreciate something like that and find it very useful. That's a very generous consideration.
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Re: Critical Analysis and Development.

Post by Jayme » Tue Aug 27, 2013 9:20 pm

We (the judges) would benefit greatly from it too. With the complete lack of competitions locally (though hopefully there will be one aside from Garrison soon - though it seems to have stalled currently), it's tricky to keep up judging skills.

Anyway - watch for a new post with more on this soon!
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Re: Critical Analysis and Development.

Post by GuingesRock » Wed Aug 28, 2013 7:26 pm

Jimmy wrote: Also, there's no need to aerate your dry yeast (unless you're repitching from a starter or slurry)
I’m very interested in this now. I’m brewing high gravity beers (usually over 8% ABV) with half a bag (27.5 lbs) of base malt in 10 gal. I read the Safeale US-05 instructions and it said to whisk vigorously to aerate ½ hour after pitching dry yeast. I also read, and was told that it was important to aerate for high ABV beers. I’m pitching 3 sachets of dry yeast. I’d still like to pitch dry yeast without rehydrating, but I think I will no longer be able to whisk after pitching as I have installed a permanent chilling coil in the pot and the coil will get in the way. Do people think I will notice a difference if I don’t whisk? Will I get the same results?
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Re: Critical Analysis and Development.

Post by CartoonCod » Wed Aug 28, 2013 8:05 pm

Here are two ideas you could follow up on:
- Try adding a very small amount of olive oil (there are other posts about this).
- Get a simple aquarium pump hooked up to a 0.2 micron inline filter

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Re: Critical Analysis and Development.

Post by GuingesRock » Wed Aug 28, 2013 8:36 pm

CartoonCod wrote:Here are two ideas you could follow up on:
- Try adding a very small amount of olive oil (there are other posts about this).
- Get a simple aquarium pump hooked up to a 0.2 micron inline filter
Thanks! I think I’ll do the olive oil thing. I read about that before, I think I even read the original study. I never thought I would become one of “those people” although perhaps I had an inkling that I might. At least I will be able to tell myself that I am doing something about it, which is half the battle. So, I dip a pin head in olive oil and dip that in the wort towards the end of the boil, right? or wrong?
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Re: Critical Analysis and Development.

Post by CartoonCod » Wed Aug 28, 2013 8:48 pm

I'm not sure of the exact concentration you need, but it's a very small amount that is for sure.

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Re: Critical Analysis and Development.

Post by chalmers » Thu Aug 29, 2013 5:01 pm

The amount you are mentioning is correct, but we always add immediately before pitching the yeast. Not sure if that is ideal, though.

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Re: Critical Analysis and Development.

Post by GuingesRock » Mon Sep 02, 2013 9:29 pm

Thanks Adam, Chris.

.............

Interesting! My sister in law was assessing my beers today. She has training in beer and wine tasting. She said I have to “watch my dishwasher”. She smelt the glasses in the cupboard all gleaming and clean and she pointed out they had a bad smell, and I noticed it too when she said that, talk about canned corn! Time for some Affresh I’d say. There are so many things to trip up a new brewer.
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Re: Critical Analysis and Development.

Post by GuingesRock » Sun Sep 15, 2013 10:54 am

I’m going through possible faults in my beer:

I’ve sorted out the sweetness, and if anything the beers are now a bit too dry. I don’t know if that improved because of better fermentation control, or making the beers a bit lower in ABV.

I think any diacetyl was present because I had a tendency to put the beer in the keezer too early and gear it up for drinking, and the yeast wasn’t getting enough chance to clean it up.

I think the slight sulphur odor was the glasses washed in a smelly dishwasher, and that’s dealt with.

I’ve been working on astringency. I now use X’s boiling water in the kegs and invert technique, and embarked on an even more rigorous sanitation neurosis. I always use a hell of a lot of hops, either late hopping of FWH so I can get a lot of flavour without going over the top with bitterness. Would that cause more astringency? Does anyone find that with massive late hopping?

I found this excellent link on common off flavours: http://www.northernbrewer.com/connect/2 ... f-flavors/" onclick="window.open(this.href);return false;
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Re: Critical Analysis and Development.

Post by Jayme » Sun Sep 15, 2013 9:43 pm

You just leave all the hops from the boil I your kettle during fermentation, right? I think that's your astringency problem. That or crushing your grain too fine would be my second guess. I suggest you start with using a hop bag to remove your hops after the boil.


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Re: Critical Analysis and Development.

Post by mr x » Sun Sep 15, 2013 9:52 pm

Not a big believer in crushing too fine causing astringency , unless it's flour. I lean towards a pH problem if it's the malt.

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Re: Critical Analysis and Development.

Post by Jimmy » Sun Sep 15, 2013 9:58 pm

I'm also skeptical that leaving the hops in during fermentation would cause astringency - I transfer the hops to the fermentor on all my brews. There was actually an experiment on one of the brewing podcasts that determined that it didn't matter if everything got transferred into the fermentor; the end product turned out the same or better with the batches that were fermented with all the hop sludge and break material transferred from the kettle.

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Re: Critical Analysis and Development.

Post by GuingesRock » Mon Sep 16, 2013 8:06 am

Thanks for the interesting thoughts everyone! It will help me get to the bottom of it.

The first thing I started doing, after reading a post by TonyL, was skimming off the hot break. I tasted that stuff from the bowl and it had mouth puckering astringency. The next thing I plan to try is skimming the yeast at high krausen. It seems to be an important thing to do when making real ale and all the real ale breweries do that.

X, I need to stop putting my head in the sand, and look into my water. I'll probably need some help with that some time, I'm a bit scared to get into it, but I better knuckle down.

Does the attached water profile mean anything to anyone please? I didn't understand it. Apparently pages #18, 20 and 22 is my water under the heading of Town Hall.
Mark what I sent is a lot more than you probably need sorry about that. Pages #18,20, and 22 under the heading of Town Hall should answer your questions. This sampling represents the distribution system.
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Last edited by GuingesRock on Mon Sep 16, 2013 2:37 pm, edited 1 time in total.
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Re: Critical Analysis and Development.

Post by GuingesRock » Mon Sep 16, 2013 1:13 pm

Is this stuff a good idea: http://www.torontobrewing.ca/servlet/th ... 5.2/Detail (PH stabilizer)
BeerSmith Home Brewing News
________________________________________
Mash pH - Water Treatment for Brewing Beer
For many years I never worried about balancing pH or even what my water profile was when brewing. After all, the beer was fine and most of the time I was brewing with extract, so pH did not matter much.
However once I started all grain brewing, the water I brewed with suddenly started to matter. It also helped that I moved to an area with extremely hard water, which forced me to use bottled water to produce anything reasonably resembling beer. It turns out that the pH of your mash has a huge impact on the mashing process as well as taste of your finished all-grain beer.
Understanding pH: Alkalinity and Acidity
Pure water has a pH of 7.0, which means that it is neither acidic nor alkaline. If you are into chemistry, this means that the free H+ (hydronium) ions are balanced with the OH- (hydroxide) ions giving equal concentrations capable of forming H2O. If water has an excess of H+ ions, we call it acidic (lower pH), while an excess of OH- ions gives us alkaline (higher pH) water.
Now it we take our pure water in the form of rain and run it down through the atmosphere and soil it picks up CO2 and Calcium from the soil, these elements will bind with the H+ ions leaving a bunch of free OH- (hydroxide) ions making our water more alkaline. This increases the pH of the water. Most tap water is slightly alkaline for this reason. Really hard water can be highly alkaline.
Interestingly all malts (and dark malts in particular) have phosphates in them that react with the calcium and magnesium ions in alkaline water freeing up H+ ions that make the mixture acidic. Adding malt, especially dark malt, lowers the pH of the malt water mixture in the mash.
The Importance of Mash pH
The pH of the mash is very important for proper conversion of sugars during the mash and also due to its effect on finished beer. Mashing should always take place at a pH between 5.1 and 5.3. However, its important to note that we are talking about the pH of the mixed mash, which as I point out above depends on the color and quantity of malts added to the beer. In most cases the mixed mash will be slightly alkaline (pH above 5.3) and require an acidic addition or buffer to bring it down to 5.2.
Though some commercial brewers can accurately predict the pH of their mash in advance, few homebrewers have the detailed knowledge and data available to do this. The problem is that the color, quantity and even type and supplier of the malt can change the pH. In addition, your starting water and its interactions with the malts may vary with each recipe. Remember that commercial brewers brew the same recipe every time using the same ingredients, while homebrewers do this only rarely.
That's why homebrewers are reduced to measuring the pH of each mash right after it is mixed and then adjusting our pH as early as possible in the mashing process.
Measuring pH can be done in several ways including pH (litmus) strips, precison pH strips and even using an electronic pH meter. Of the three methods, precision pH strips are usually most cost effective and practical. Standard pH strips lack the precision needed to measure down to a tenth of a point pH, and electronic meters are expensive and require frequent replacement of the electrodes to maintain accuracy.
Another practical consideration is that the mash is usually hot, so you need to adjust the pH reading for temperature. Hot wort will almost always provide a higher pH reading than the actual wort. You can compensate for this either by rapidly cooling the sample to room temperature before measuring or applying a correction factor after taking the reading. Check the documentation with your pH strips to determine the appropriate correction.
Methods for Adjusting Mash pH
There are several methods available to the homebrewer for adjusting the pH of your wort. As noted earlier, in most cases you will need to lower your pH to reach the 5.2 target level.
• Calcium and Magnesium Salts: Three salt: Gypsum (CaSO4), Epsom Salt (MgSO4) and Calcium Chloride (CaCl) can be added to lower your pH. The calcium and magnesium ions in these additions reduce the alkalinity of the water. Note, however, that the sulfate and chloride ions react with the phosphates from the mash, which can lead to undesirable flavors. As a result you need to limit the amount added. You can calculate appropriate amounts using a water tool such as the one in BeerSmith. Suggested limits are 50-150 ppm for calcium, 50-150 ppm for sulfate, 0-150 ppm for chloride and 10-30 ppm for magnesium. See our article on water profiles for more information.
• Food Grade Acids - Acid additions counter the H+ ion and directly lower the alkalinity of the mash. Popular additions include phosphoric acid, sulfuric acid and lactic acid. All of these contribute other flavors and ions to the beer as well, which can again cause problems if used in excessive amounts. Phosphoric acid is used to make soda, and will contribute phosphates to the mash. Lactic acid will add lactates, and is used in many Belgian styles to sour the beer. Sulfuric acid will contribute sulfates. In general you should add the minimum needed to achieve your target pH. The amount will vary depending on the concentration of your acid and wort volume.
• Acid Malt - Because of German purity laws (the Reinheitsgebot) that prevent additives to German beer, sour malt (called acid malt) is used to aid in the brewing of light beers to lower mash pH. Acid malt is made by souring malt with lactic bacteria for a short period which effectively creates lactic acid. Adding acid malt is effectively equivalent to adding lactic acid to the mash. Adding one percent of acid malt effectively lowers the pH of the malt by approximately 0.1 pH.
• Sour Mash - Another technique developed by the Germans is to create a sour mash which again contains lactic acid produced by lactic bacteria. The technique is to mash a quantity of grain, cools it to about 80F and then adds some fresh malt (which contains lots of lactic bacteria naturally) and lets the mixture sit overnight. The bacteria will quickly sour the mash and start fermenting it, again creating lactic acid. The next day this sour mash can be mixed with a regular mash to lower its pH. The challenge with sour mashing is that it can be somewhat inconsistent in pH and also labor intensive.
• Acid Rest - Though seldom used today thanks to modern highly modified malts, an acid rest in the 95F (35C) range can break down phytins in the malt into phytic acid that will lower the mash pH. This was traditionally done in German triple decoction mashes, and is most effective when used with undermodified malts.
5.2 Stabilizer - A number of brew stores now carry an additive called 5.2 stabilizer. This is a powder you can add to the beer to lower the mash pH to 5.2. It consists of buffers that reduce the alkalinity of the mash to reach a 5.2 level. As long as your starting water is not completely out of kilter, this is a good simple solution for many homebrewers.


Brad Smith
BeerSmith.com

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Re: Critical Analysis and Development.

Post by mr x » Mon Sep 16, 2013 2:03 pm

I had some of that at one time, but found I didn't need it. Don't think it would hurt to try it.
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Re: Critical Analysis and Development.

Post by dean2k » Mon Sep 16, 2013 2:20 pm

GuingesRock wrote:..... I tasted that stuff from the bowel and it had mouth puckering astringency.
No wonder. Found your problem right there.
.............................................

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Re: Critical Analysis and Development.

Post by GuingesRock » Mon Sep 16, 2013 2:35 pm

dean2k wrote:
GuingesRock wrote:..... I tasted that stuff from the bowel and it had mouth puckering astringency.
No wonder. Found your problem right there.

BOWL! but it tasted like it came from the bowel.

:lol:

Found a good thread on 5.2. Might not be all it's cracked up to be: http://hbd.org/discus/messages/26895/28079.html
Last edited by GuingesRock on Mon Sep 16, 2013 8:40 pm, edited 2 times in total.
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Re: Critical Analysis and Development.

Post by Rathers » Mon Sep 16, 2013 3:00 pm

Hey,

Not to go into to much detail but a low pH of 5.2 would only really be done by British brewers. Most North American brewers and German brewers would aim for a higher pH.

The calcium ions from the salts used by British brewers acts like a buffer. So in the UK its common to add acid to the hot liquor to remove stuff and then add salts to get the water right. Germans would see this as a bit odd and aim for a higher pH due to the lack of salts in their mashes.

Cheers,

Andrew

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Re: Critical Analysis and Development.

Post by GuingesRock » Mon Dec 09, 2013 7:40 am

From here: http://www.brewnosers.org/forums/viewto ... 459#p79459" onclick="window.open(this.href);return false; (Weizen thread)
NASH wrote: Treat the water appropriately for ion concentrations and PH levels.


I’ve been putting my head in the sand with this one. But I have to start working on it. I have the water book, some ph testing strips and got the town water profile (attached), but that’s as far as I got. Does anyone have any tips or advice for the uninitiated please. The water is also passing through a carbon filter. Does that change its profile?
Mark what I sent is a lot more than you probably need sorry about that. Pages #18,20, and 22 under the heading of Town Hall should answer your questions. This sampling represents the distribution system.
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Re: Critical Analysis and Development.

Post by GAM » Mon Dec 09, 2013 10:06 am

There is a spread sheet that you fill in your target ion/PH amounts (it was posted some time ago) ,then add chalk/salt etc to get to the range you want. I did it once and because I only brew English styles I use the same additions every time.

I think it was Mr.X who posted the SS.

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Re: Critical Analysis and Development.

Post by GAM » Mon Dec 09, 2013 12:22 pm

This.
EZ_water_calculator_3.0.2.xls
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Re: Critical Analysis and Development.

Post by adams81 » Mon Dec 09, 2013 1:14 pm

Is this similar to the water profile tool in Beersmith?

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